AMI Micro-300 Series BET Surface Area and Pore Size Analyzer
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The AMI 300 Series can accurately produce surface area and pore size results of powder materials. According to the different test functions, this series of instruments are divided into three types, there are A, B, and C. Every analysis station has its own dedicated dosing manifold for optimal analysis duration. The C type is configured with 1 torr or 0.1 torr high-sensitive pressure sensors and turbo molecular pump with ultimate pressure of 10-8 Pa. The three analysis stations can also be used for in-situ sample preparation to avoid sample contamination. It can effectively take microporous analysis of microporous materials such as molecular sieve, catalyst, activated carbon, and other microporous materials.
Hardware and Operation
Vacuum System
Techniques
Clear tabular reports include
Features
Internal temperature of test module can be controlled through Real-time monitoring, ensuring accuracy of adsorption detection.
Micro 300C with 1torr (selectable 0.1torr) makes the partial pressure of P/P0 up to 10-7 – 10-8 (N2/77K) in the physical adsorption analysis.
Using independent P0 pressure sensor for P0 value by inching test, guarantees the reliability of experimental data. Atmospheric pressure input
Specifications
Feature Meso 300A Micro 300B Micro 300C
Adsorbed Gas Non corrosive gases, such as N2, Ar, Kr, H2, O2, CO2, CO, NH3, CH4, etc.
Pressure Sensor at
Analysis Station
1000 torr, 3 1000 torr, 3;
10 torr, 1 (optional 2 or 3);
1 torr(0.1torr can be selected),1 (optional 2 or 3)
1000 torr, 3;
10 torr, 3;
1 torr (0.1torr can be selected), 3
Accuracy: ±0.15% (F.S.)
Pressure Sensor at P0 Station 1000 torr,3
(Accuracy: ±0.15% (F.S.)
Degas System The standard configuration is 3 stations in-situ degassing, which can simultaneously degas 3 samples under vacuum heating;
Another optional external 4-station vacuum heating degassing machine;
Degas Temperature Ambient to 400 ℃. Free to set up target temperature.
Cold Trap 1
Vacuum Pump Two-stage rotary vane mechanical
vacuum pump,
the ultimate pressure is
6.7*10-2 Pa
Two-stage rotary vane mechanical
vacuum pump, the ultimate
pressure is 6.7*10-2 Pa, optional turbo
molecular pump
Turbo molecular pump (ultimate pressure 10-8 Pa) and front
mechanical vacuum pump
(ultimate pressure is 6.7*10-2 Pa)
Analysis Port Samples on the 3 analysis bits can be tested at same time (including P0 test).
Test Principle Gas adsorption by static-volumetric analysis
Measurement Range of
Specific Surface Area
0.0005 m2/g to the infinity;
Standard sample repeat accuracy is less than ± 1.0%
0.0001m2/g to the infinity;
Standard sample repeat accuracy is less than ± 1.0%
0.0001m2/g to the infinity;
Standard sample repeat accuracy is less than ± 1.0%
Test Range of Pore Diameter 0.35 nm-500 nm; Pore dimension repeatability is less than 0.2 nm in the accurate analysis of materials with pore size greater than 2 nm 0.35 nm-500 nm; Pore dimension repeatability is less than 0.02 nm in the accurate analysis of micropore 0.35 nm-2 nm 0.35 nm-500 nm; Pore dimension repeatability is less than 0.02 nm in the accurate analysis of micropore 0.35 nm-2 nm
Minimum Pore Volume 0.0001 cm3/g
Range of Relative Pressure P/P0 10-5-0.998 10-6/10-8-0.998 10-8-0.998
Overall Dimension Depth: 870 mm; width: 570 mm; height: 890 mm; weight: 80 Kg -90 Kg
Ambient Temperature 15-40 oC
Related Humidity 30%-60%
Electrical Supply AC220 V ± 20 V, 50/60 HZ, maximum power 300W;
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